Characterization and process optimization of Melastoma malabathricum l. extract / (Record no. 3114)

MARC details
000 -LEADER
fixed length control field 03985nam a2200265 a 4500
001 - CONTROL NUMBER
control field vtls000058696
003 - CONTROL NUMBER IDENTIFIER
control field KUKTEM
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251114204511.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 120316t2011 my a f m 001 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0003986(Local)
039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE]
Level of rules in bibliographic description 201905150924
Level of effort used to assign nonsubject heading access points fauzi
Level of effort used to assign subject headings 201710041235
Level of effort used to assign classification aishah
-- 201203161128
-- ida
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) TP156.E8 D47 2011 rs Thesis
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Dessy Ambarwati
245 10 - TITLE STATEMENT
Title Characterization and process optimization of Melastoma malabathricum l. extract /
Statement of responsibility, etc. Dessy Ambarwati
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Kuantan, Pahang :
Name of publisher, distributor, etc. UMP,
Date of publication, distribution, etc. 2011
300 ## - PHYSICAL DESCRIPTION
Extent xxii, 134 p. :
Other physical details ill. (some col.) ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
502 ## - DISSERTATION NOTE
Dissertation note Thesis (Master of Engineering (Chemical Engineering)) -- Universiti Malaysia Pahang - 2011
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Bibliography : p. 84-95
520 3# - SUMMARY, ETC.
Summary, etc. Melastoma malabathricum L. (MML) or local name as senduduk, have demonstrated the presence of phenolic compound. The phenolic compound in plants has a role to inhibiting the growth of microorganism. Antimicrobial activity in plants has become an important area in the food and beverages industry; therefore natural preservatives will be very potential for more natural and fresh-like foods. In this study, to obtain the phenolic compound from MML was used extraction. Conventional extraction as heating, boiling, or refluxing can be used to extract phenolic, however, the disadvantages are the loss of phenolics due to ionisation, hydrolysis and oxidation during extraction as well as the long extraction time. In this thesis, the potentionals of ultrasonic technology in extraction was investigated. Comparation between ultrasonic-assisted extraction and classical extraction (homogenizer extraction) with incubated waterbath as a control were investigated to provide understandings of influence of ultrasonic irradiation on the production of phenolic compound in MML. Extracts were analyzed for phenolic compound (gallic acid, ellagic acid and total phenols compound). Folin Ciocalteau method was chosen for total phenols determination, while the phenolic acids (gallic acid and ellagic acid) were analyzed by using HPLC. Results showed that ultrasonic-assisted extraction was more effective to produce phenolic compound (gallic acid, ellagic acid and total phenol) from MML extract than using the classical extraction.. Acid-hydrolysis method was found the best method for post-treatment process of MML extract to produce maximum phenolic compound. Some characterization studies also investigated to understandings about nutrient composition, chemical properties and antimicrobial activity of MML extract. MML extract showed inhibitory activity against microorganism, such as B. cereus, B. subtilis, S. typhi and E. coli. The extraction process of MML extract were studied in this thesis, namely solid-to-liquid ratio, extraction temperature and extraction time. Prior to conducting an experimental design approach, in this study was indentification the parameter range in extraction process. The experimental run and optimization were designed using Design Expert Software as suggested by Response Surface Methodology (RSM). The optimum extraction process for highest phenolic compound extracted were obtained at extraction temperature and extraction time of 59.96 °C and 92.55 min, respectively, whereas, the solid loading about 20.07 g. Under this condition, the yield of gallic acid, ellagic acid and total phenol was 1.79 mg/g, 0.16 mg/g and 15.10 mg GAE/g. The results obtained in this study have exposed capability of ultrasonic technology in extraction of phenolic compound. Further works are nevertheless required to provide deeper understanding the mechanisms involved to facilitate the development of an optimum system applicable to the industry.
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Extraction (Chemistry)
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Phenols
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://ecollib.ump.edu.my/3904/">http://ecollib.ump.edu.my/3904/</a>
Public note Library access only
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Home library Current library Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost Library of Congress Classification   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   TP156.E8 D47 2011 rs Thesis 0000063424 04/09/2019 1 04/09/2019 Thesis
  Not lost Library of Congress Classification   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   CD 5978 | TP156.E8 D47 2011 rs Thesis 0000063425 04/09/2019 1 04/09/2019 Thesis

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