MARC details
| 000 -LEADER |
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| fixed length control field |
04045ntm a2200373 i 4500 |
| 001 - CONTROL NUMBER |
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| control field |
vtls000105339 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
KUKTEM |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20251114204522.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
180928t20182018my da f a m 001 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
THE0000829(Local) |
| 039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE] |
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| Level of rules in bibliographic description |
201905271213 |
| Level of effort used to assign nonsubject heading access points |
nazirah |
| -- |
201809281025 |
| -- |
fateeha |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
UMP |
| Language of cataloging |
eng |
| Transcribing agency |
UMP |
| Description conventions |
rda |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) |
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| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) |
FKKSA .A363 2018 r Thesis |
| 100 0# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Nurul Akma Reduan, |
| Relator term |
author. |
| 245 10 - TITLE STATEMENT |
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| Title |
Synthesis and characterization of silver nanoparticles filled epoxy composite / |
| Statement of responsibility, etc. |
Nurul Akma Reduan |
| 264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
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| Place of production, publication, distribution, manufacture |
Kuantan, Pahang : |
| Name of producer, publisher, distributor, manufacturer |
UMP, |
| Date of production, publication, distribution, manufacture, or copyright notice |
2018 |
| 264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
|---|
| Date of production, publication, distribution, manufacture, or copyright notice |
© 2018 |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
xvi, 125 pages : |
| Other physical details |
illustrations (some color), charts ; |
| Dimensions |
30 cm. + |
| Accompanying material |
1 CD-ROM |
| 336 ## - CONTENT TYPE |
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| Content type term |
text |
| Source |
rdacontent |
| 336 ## - CONTENT TYPE |
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| Content type term |
text |
| Source |
rdacontent |
| 337 ## - MEDIA TYPE |
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| Media type term |
unmediated |
| Source |
rdamedia |
| 337 ## - MEDIA TYPE |
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| Media type term |
computer |
| Source |
rdamedia |
| 338 ## - CARRIER TYPE |
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| Carrier type term |
volume |
| Source |
rdacarrier |
| 338 ## - CARRIER TYPE |
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| Carrier type term |
computer disc |
| Source |
rdacarrier |
| 347 ## - DIGITAL FILE CHARACTERISTICS |
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| File type |
text file |
| Encoding format |
PDF |
| Source |
rda |
| 500 ## - GENERAL NOTE |
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| General note |
Faculty of Chemical & Natural Resources Engineering |
| 502 ## - DISSERTATION NOTE |
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| Dissertation note |
Thesis (Master of Engineering (Chemical)) -- Universiti Malaysia Pahang – 2018 |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc. note |
Includes bibliographical references |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc. |
In this study, silver nanoparticles (AgNPs) were successfully synthesized via chemical reduction method. Silver nitrate (AgNO3), was used as a precursor, Sodium Borohydride (NaBH4) as a reducing agent and Cetyltrimethylammonium Bromide (CTAB) as a surfactant. The effect of reaction temperature, concentration of AgNO3 and NaCl were investigated in order to synthesize AgNPs with uniform shape and narrow particles distribution. The synthesized AgNPs was characterized by UV-VIS, TEM, XRD, and FESEM while; the average size was measured by Image-J software. XRD diffraction peak confirm that the samples prepared are AgNPs based on the peak position at 38.4° and 44.8°. Synthesis parameter at 60°C, 1.00 mM and 3.0 mM of reaction temperature, concentration of AgNO3 and NaCl respectively shows an optimum condition which produced AgNPs with narrow particle distribution, no agglomeration and uniform spherical shape at the end of reaction. The addition of NaCl affected the state of the reaction solution which is pH. This study shows solution at pH 7.5 gave better particles formation with no appearance of agglomerated particles. Meanwhile, stability study by UV-Vis and TEM analysis shows that the as-synthesized AgNPs was remain stable up to 1 month. The implementation of aqueous to organic phase transfer technique in this study is aimed to improve particles dispersivity in the epoxy polymeric system (composite preparation). FESEM analysis showed the AgNPs were dispersed well in the epoxy system. The composites of epoxy and AgNPs composite were fabricated as a function of particles concentration in the volume percentage (vol %) on thermal and thermo-mechanical properties of composite. Incorporation of AgNPs in the epoxy system is aimed to improve the thermal and thermo-mechanical properties of the resultant composite. The thermal and thermo-mechanical properties from TGA, DSC and DMA analysis shows that AgNPs- filled epoxy composite have higher thermal and thermo-mechanical properties compared to unfilled epoxy polymer. TGA analysis showed that, sample at 1.0 vol % AgNPs was recorded in the highest value of thermal properties compared to the unfilled AgNPs. From DMA analysis, samples at 0.2 vol% shows the thermo-mechanical properties of AgNPs-filled epoxy composite obtained 47-56% increment in the storage modulus and tan delta compared to unfilled AgNPs epoxy composite. Based on experimental results, thermal and thermo-mechanical can be conclude that AgNPs-filled epoxy composite can be used either in engineering or in various applications. |
| 610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME |
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| Corporate name or jurisdiction name as entry element |
Faculty of Chemical & Natural Resources Engineering |
| General subdivision |
Dissertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
Universities and colleges |
| General subdivision |
Disertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
Theses |