Kinetic study of esterification of fatty acids over calcium ferrite catalyst / (Record no. 5457)

MARC details
000 -LEADER
fixed length control field 03041ntm a2200277 a 4500
001 - CONTROL NUMBER
control field vtls000084866
003 - CONTROL NUMBER IDENTIFIER
control field KUKTEM
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251117113241.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 150114t2014 my a f m 000 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0004617(Local)
039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE]
Level of rules in bibliographic description 201905171000
Level of effort used to assign nonsubject heading access points azhar
Level of effort used to assign subject headings 201712051640
Level of effort used to assign classification huda
-- 201501141538
-- fawwaz
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) TP359.B46 F38 2014 r Bc.
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Nurul Fatihah Mahamad Roli
245 10 - TITLE STATEMENT
Title Kinetic study of esterification of fatty acids over calcium ferrite catalyst /
Statement of responsibility, etc. Nurul Fatihah Mahamad Roli
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Kuantan, Pahang :
Name of publisher, distributor, etc. UMP,
Date of publication, distribution, etc. 2014
300 ## - PHYSICAL DESCRIPTION
Extent xv, 42 p. :
Other physical details ill. ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
500 ## - GENERAL NOTE
General note Faculty of Chemical & Natural Resources Engineering
502 ## - DISSERTATION NOTE
Dissertation note Project paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang – 2014
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Bibliography : p. 36-38
520 3# - SUMMARY, ETC.
Summary, etc. Biodiesel is a promising renewable alternative fuel to fossil energy. For the biodiesel production from non-edible oil feedstocks like Jatropha curcas oil, a pre-treatment step is essential, which is the esterification of free fatty acids in the feedstocks in order to avoid soap formation and minimize catalyst deactivation. The FFA used in this experiment was obtained by two methods which saponification, where oil (Jatropha oil) is converting to soap and also acidification, where the sodium salts of free fatty acids are converted to FFA by using hydrochloric acid (HCL). In this research, Calcium Ferrite (CaFe2O4) catalyst was prepared for the esterification of FFA. Due to its ability as an effective catalyst and without changing its crystal structure, Calcium Ferrite can yield high conversion of FFA into biodiesel. Calcium Ferrite catalyst was synthesized by Pechini method. Pechini process was newly used in this field of catalyst production. It is a powder-synthesis process that involves the formation of a polymeric precursors (resin), using citric acid and ethylene glycol. The molar ratio for citric acid monohydrate to ethylene glycol used in this experiment was 60:40. The calcinations behavior of the precursor powders of Calcium Ferrite was studied in the temperature range of 450-12000C in an air atmosphere. Characterization of the powder samples were performed using several processes including X-ray diffractometry (XRD), thermogravimetry (TGA) and Brunauer Emmett Teller (BET) analyzer. The effects of reaction temperature, methanol/FFA molar ratio, catalyst concentration on the FFA conversion were also studied. Based on the findings of this study, ethanol to FFA ratio of 30:1, 10 % weight of the catalyst, reaction time of 6 h and temperature 70 0C were found as the optimum for the esterification reaction. Therefore, the developed catalyst could be effectively used for the esterification of FFA in plant oil
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Biodiesel fuels
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Esterification
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://ecollib.ump.edu.my/18331/">http://ecollib.ump.edu.my/18331/</a>
Public note Access in library only
Holdings
Withdrawn status Lost status Damaged status Not for loan Home library Current library Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   TP359.B46 F38 2014 r Bc. 0000091657 04/09/2019 1 04/09/2019 Final Year Report
  Not lost   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   CD 8595 | TP359.B46 F38 2014 r Bc. 0000091658 04/09/2019 1 04/09/2019 Final Year Report

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