Synthesis and characterization of hard kappa carrageenan capsule through glyoxal and glyoxylic acid crosslinking / (Record no. 5871)

MARC details
000 -LEADER
fixed length control field 02737ntm a2200265 a 4500
001 - CONTROL NUMBER
control field vtls000084709
003 - CONTROL NUMBER IDENTIFIER
control field KUKTEM
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251117113254.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 141224t2014 my a f m 000 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0004720(Local)
039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE]
Level of rules in bibliographic description 201905141025
Level of effort used to assign nonsubject heading access points smfh
Level of effort used to assign subject headings 201905141025
Level of effort used to assign classification smfh
Level of effort used to assign subject headings 201712041028
Level of effort used to assign classification huda
-- 201412241654
-- fawwaz
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) TP363 .I58 2014 r Bc.
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Intan Lyana Ahmad
245 10 - TITLE STATEMENT
Title Synthesis and characterization of hard kappa carrageenan capsule through glyoxal and glyoxylic acid crosslinking /
Statement of responsibility, etc. Intan Lyana Ahmad
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Kuantan, Pahang :
Name of publisher, distributor, etc. UMP,
Date of publication, distribution, etc. 2014
300 ## - PHYSICAL DESCRIPTION
Extent xiii, 82 p. :
Other physical details ill. ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
500 ## - GENERAL NOTE
General note Faculty of Chemical & Natural Resources Engineering
502 ## - DISSERTATION NOTE
Dissertation note Project paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang – 2014
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Bibliography : p. 62-67
520 3# - SUMMARY, ETC.
Summary, etc. This research is about the synthesis and characterization studies of the hydrogel for hard kappa carrageenan capsule through glyoxal and glyoxylic acid crosslinking. In this work, kappa carrageenan hydrogel were prepared by chemical crosslinking using glyoxal and glyoxylic acid as the crosslinking agent and hydrochloric acid (HCl) as the catalyst. The purpose of this study is to select the best crosslinker material to develop hard kappa carrageenan capsule that can improve its propertis through molecular recognition approach by using crosslink technique. Aqueous kappa carrageenan (3% w/v) was reacted with a certain amount of glyoxal and glyoxylic acid (25%) respectively and HCl (0.1N) at 40°C. After 30 minutes of reaction, the homogenous solution was cooled at room temperature producing gel form. The gel was soaked in the ethanol to remove unreacted residue or chemicals. The obtained hydrogel was air dried at room temperature to constant weight. The FTIR spectra, DSC, TGA and the value of swelling ratio of obtaining hydrogel showed that kappa carrageenan could be crosslinked using glyoxal or glyoxylic acid. Based on the FTIR, there were some functional group detected showed that the crosslinker and kappa carrageenan was successsful crosslinked. There were no significant differences in the swelling degree of hydrogel synthesized in the distilled water and all buffer solution. The crosslinking with a certain amount of glyoxal and HCl may be produce hydrogel with a lower swelling degree. The kappa carrageenan hydrogel was found to be pH sensitive, indicating a high potential to be used in drg delivery polymer system
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Carrageenan
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://ecollib.ump.edu.my/18389/">http://ecollib.ump.edu.my/18389/</a>
Public note Access in library only
Holdings
Withdrawn status Lost status Damaged status Not for loan Home library Current library Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   TP363 .I58 2014 r Bc. 0000091673 04/09/2019 1 04/09/2019 Final Year Report
  Not lost   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   CD 8603 | TP363 .I58 2014 r Bc. 0000091674 04/09/2019 1 04/09/2019 Final Year Report

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