Optimizing isotactic polypropylene membrane preparation condition via tips for carbon dioxide and nitrogen separation / (Record no. 6722)

MARC details
000 -LEADER
fixed length control field 03917nam a2200289 a 4500
001 - CONTROL NUMBER
control field vtls000097824
003 - CONTROL NUMBER IDENTIFIER
control field KUKTEM
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251117113324.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 160920t2016 my da f ah 000 0 eng|d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0001057(Local)
039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE]
Level of rules in bibliographic description 201905171314
Level of effort used to assign nonsubject heading access points nazirah
Level of effort used to assign subject headings 201710171126
Level of effort used to assign classification aishah
-- 201609201225
-- safura
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) FKKSA .Z85 2016 r Thesis
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Wan Zulaisa Amira Bt Wan Jusoh
245 10 - TITLE STATEMENT
Title Optimizing isotactic polypropylene membrane preparation condition via tips for carbon dioxide and nitrogen separation /
Statement of responsibility, etc. Wan Zulaisa Amira Bt Wan Jusoh
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. Kuantan, Pahang :
Name of publisher, distributor, etc. UMP ,
Date of publication, distribution, etc. 2016
300 ## - PHYSICAL DESCRIPTION
Extent xvii, 337 p. :
Other physical details col. ill. ;
Dimensions 30 cm. +
Accompanying material 1 CD ROM
500 ## - GENERAL NOTE
General note Faculty of Chemical and Natural Resources Engineering
502 ## - DISSERTATION NOTE
Dissertation note Thesis (Master of Engineering (Chemical) -- Universiti Malaysia Pahang – 2016
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Bibliography : p. 335 - 337
520 3# - SUMMARY, ETC.
Summary, etc. Over the past few decades, the emission of the flue gases into the atmosphere has increased and warms the earth’s surface. One of the options to minimize this problem is by recovering carbon dioxide (CO2) from flue gas before releasing it to surrounding. Gas separation technology using membrane is a simple system that can effectively remove the CO2 from flue gas as well as offering low installation cost. However, in the flue gas, there is water vapour content that causes the membrane to swell. Thus, for this study, in order to increase the durability and performance of membrane for CO2 and nitrogen (N2) separation, the hydrophobic membrane is proposed. This study focuses on the effect of the addition of adipic acid on the hydrophobicity of the isotactic polypropylene (iPP) membranes. Response Surface Method (RSM) consists of 2-Level Factorial (FFD) and Centre Composite Design (CCD) for screening and optimization processes in the production of iPP microporous membrane were performed respectively. From this study, it was found that there are no such work has been reported in the open literature on the optimization of iPP membrane for gas separation. For morphology by using Scanning Electron Microscopy (SEM), observation on the iPP- DPE membranes exhibited smaller pore size compared to iPP-Methyl Salicylate (MS) membrane. Meanwhile, increasing adipic acid showed decreasing membrane pore size distribution. The result obtained by Fourier Transform Infrared Spectroscopy (FTIR) showed that there is no bonding changes between raw iPP and membrane fabricated by Thermally Induced Phase Separation Method (TIPS). Membrane prepared by Dipenyl Ether (DPE) and without addition of adipic acid produced the highest contact angle, CO2 permeability and selectivity which are 112°, 22.01 GPU and 1.59 respectively. Analysis of variance of FFD showed that the impact of drying temperature and drying time were important than polymer concentration and immersion time in methanol toward contact angle and selectivity. The optimum membranes prepared in this experiment were membranes with the contact angle value and selectivity of 106.49 ° and 1.96 respectively at drying temperature of 54.96 °C and drying time of 18.66 min. These drying temperature and time are adequate for total methanol evaporation from pores which contributed to high selectivity and high contact angle value. The low error (below 30%) between predicted and actual value indicating that regression equations obtained from the FFD and CCD were expected to apply in the preparation of iPP membranes, can reasonably predict and optimize the performance of the iPP membranes
610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Faculty of Chemical and Natural Resources Engineering
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Universities and Colleges
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Theses
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="http://ecollib.ump.edu.my/3523/">http://ecollib.ump.edu.my/3523/</a>
Public note Library access only
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Home library Current library Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost Library of Congress Classification   Final Processing UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   FKKSA .Z85 2016 r Thesis 0000111087 04/09/2019 1 04/09/2019 Thesis
  Not lost Library of Congress Classification   Final Processing UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   CD 9901 | FKKSA .Z85 2016 r Thesis 0000111088 04/09/2019 1 04/09/2019 Thesis

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