MARC details
| 000 -LEADER |
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| fixed length control field |
02913ntm a2200289 a 4500 |
| 001 - CONTROL NUMBER |
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| control field |
vtls000100037 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
KUKTEM |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20251117113333.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
170504t2017 my da f abm 000 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
THE0000881(Local) |
| 039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE] |
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| Level of rules in bibliographic description |
201905271453 |
| Level of effort used to assign nonsubject heading access points |
nazirah |
| Level of effort used to assign subject headings |
201710041249 |
| Level of effort used to assign classification |
aishah |
| -- |
201705041433 |
| -- |
saini |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
UMP |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) |
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| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) |
FKKSA .F38 2017 r Thesis |
| 100 0# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Fatimah Azzahra’ Misebah |
| 245 10 - TITLE STATEMENT |
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| Title |
Kinetics of biolubricant synthesis from jatropha curcas oil using Paphia undulata as a solid catalyst / |
| Statement of responsibility, etc. |
Fatimah Azzahra’ Misebah |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. |
|---|
| Place of publication, distribution, etc. |
Kuantan, Pahang : |
| Name of publisher, distributor, etc. |
UMP, |
| Date of publication, distribution, etc. |
2017 |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
xiv, 150 p. : |
| Other physical details |
ill. (some col.) ; |
| Dimensions |
30 cm. |
| 500 ## - GENERAL NOTE |
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| General note |
Faculty of Chemical & Natural Resources Engineering |
| 502 ## - DISSERTATION NOTE |
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| Dissertation note |
Thesis (Master of Engineering in Chemical) -- Universiti Malaysia Pahang – 2017 |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc. note |
Bibliography : p. 86-97 |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc. |
Nowadays, there is growing concern in looking for a renewable source of lubricant due to increasing demand for industrial applications besides depletion of world petroleum resource with uncertainty in petroleum supply has stimulated the search for biolubricants as an environmental friendly alternative source. Therefore, the research has been done using Jatropha curcas oil for biolubricant as new source over derived calcium oxide from Papia undulata shell as a solid catalyst. In addition, the research aims to determine the kinetic reaction for transesterification of Jatropha curcas oil on biolubricant yield. The first step in the research method was esterification process of free fatty acid (FFA) in Jatropha curcas oil, for reduction of the free fatty acid value and production of Jatropha curcas oil metyl ester (JCOME). This was followed by the synthesis of lubricant from blending JCOME with TMP by evaluating the process conditions. The final products were analyzed using gas chromatography mass spectorophotometer (GCMS) for JCOME production and gas chromatography with Flame Ionization Detector (GC-FID) for Jatropha biolubricant production. The optimum reaction for JCOME production was found to be at methanol/oil ratio of 6:1, catalyst amount of 4 wt.%, temperature of 60 oC and reaction time of 3 hours with the highest yield being 93.33%. Meanwhile Jatropha biolubricant optimum conditions were at 110 0C, 3 h, 4:1 of JME: TMP and 3% w/w of catalyst with 96.66% of TMP conversion and 78.67% of TE composition. The reaction was determined to fit the second order kinetics model with overall rate constant of 0.0427 (%w/w min °C)-1 and activation energy of 2.2 kJ/mol. |
| 610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME |
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| Corporate name or jurisdiction name as entry element |
Faculty of Chemical & Natural Resources Engineering |
| General subdivision |
Dissertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
Universities and Colleges |
| General subdivision |
Dissertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name entry element |
Theses |
| 856 40 - ELECTRONIC LOCATION AND ACCESS |
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| Uniform Resource Identifier |
<a href="http://ecollib.ump.edu.my/25863/">http://ecollib.ump.edu.my/25863/</a> |
| Public note |
Library access only |