Preparation and characterisation of MgO nanoparticle incorporated bioresin using palm oil / (Record no. 7292)

MARC details
000 -LEADER
fixed length control field 03691ntm a2200373 i 4500
001 - CONTROL NUMBER
control field vtls000102853
003 - CONTROL NUMBER IDENTIFIER
control field KUKTEM
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251117113345.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 180125s2017 my a f am 000 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0000890(Local)
039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE]
Level of rules in bibliographic description 201905271504
Level of effort used to assign nonsubject heading access points nazirah
Level of effort used to assign subject headings 201802201242
Level of effort used to assign classification saini
-- 201801251055
-- saini
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
Language of cataloging eng
Transcribing agency UMP
Description conventions rda
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) FKKSA .G36 2017 r Bc.
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Gan, Wei Teng,
Relator term author.
245 10 - TITLE STATEMENT
Title Preparation and characterisation of MgO nanoparticle incorporated bioresin using palm oil /
Statement of responsibility, etc. Gan Wei Teng
264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Kuantan, Pahang :
Name of producer, publisher, distributor, manufacturer UMP,
Date of production, publication, distribution, manufacture, or copyright notice 2017
264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Date of production, publication, distribution, manufacture, or copyright notice © 2017
300 ## - PHYSICAL DESCRIPTION
Extent xiv, 60 pages :
Other physical details illustrations (some color) ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
337 ## - MEDIA TYPE
Media type term unmediated
Source rdamedia
337 ## - MEDIA TYPE
Media type term computer
Source rdamedia
338 ## - CARRIER TYPE
Carrier type term volume
Source rdacarrier
338 ## - CARRIER TYPE
Carrier type term computer dics
Source rdacarrier
347 ## - DIGITAL FILE CHARACTERISTICS
File type text file
Encoding format PDF
Source rda
500 ## - GENERAL NOTE
General note Faculty of Chemical & Natural Resources Engineering
502 ## - DISSERTATION NOTE
Dissertation note Project Paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang – 2017
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references
520 3# - SUMMARY, ETC.
Summary, etc. Alkyd resins are the product derivation of polyacid and polyol modified with monobasic fatty acid through polycondensation. Over the recent years, alkyd resins are widely used as the binder for composite and film-forming agent in paints. Vegetable oils were being explored and evaluated to synthesis alkyd resin due to its biodegradability and renewability. Synthesis of alkyd resins involved the alcoholysis of the oil by the polyol (commonly glycerol) and followed by polyesterification with a polyacid (commonly phthalic anhydride). Generally, a homogeneous or heterogeneous base catalyst was used to carry out the reaction. Nanoparticles were said to be a promising catalyst and colloidal form of nanoparticles was discovered in this context. In this work, palm oil based alkyd resin was synthesized over Magnesium Oxide (MgO) nano sol. Colloidal MgO nanoparticles were synthesised in glycerol and subsequently was used in alkyd resin synthesis. The alcoholysis process was conducted in the presence of various concentration of MgO (0.01, 0.02, 0.04 and 0.06wt% w.r.t. palm oil) at 240oC. The monoglycerides yield was found to achieve up to 95% in 40 minutes reaction time for 0.04wt% MgO catalysed system. As for the polyesterification process, fusion method was used since it was seldom discovered by other researchers. The crystallized size of the nanoparticle in sol was analysed by X-ray diffraction technique (XRD). Formation of the alkyd resin was monitored by measuring the acid values at different reaction time. Alkyd resins obtained after polyesterification of the alcoholysis products with phthalic anhydride at 240oC were characterized by employing Fourier Transform Infrared (FTIR) and Nuclear magnetic resonance (NMR) spectroscopy. The antimicrobial activity of MgO incorporated alkyd resin against microorganisms was tested via the Kirby–Bauer method. The MgO incorporated in alkyd resin not only reduced the reaction time but also was also proved to be an effective antibacterial agent which added value to the alkyd resin synthesised. Overall, MgO nanoparticles incorporated alkyd resin showed outstanding performance compared to conventional homogeneous base catalyzed system.
610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Faculty of Chemical & Natural Resources Engineering
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Universities and Colleges
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Theses
Holdings
Withdrawn status Lost status Damaged status Not for loan Home library Current library Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   FKKSA .G36 2017 r Bc. 0000122244 04/09/2019 1 04/09/2019 Final Year Report
  Not lost   Not for loan UMPLIB GAMBANG UMPLIB GAMBANG 04/09/2019   CD 11202 | FKKSA .G36 2017 r Bc. 0000122245 04/09/2019 1 04/09/2019 Final Year Report

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