MARC details
| 000 -LEADER |
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| fixed length control field |
03462ntm a2200397 i 4500 |
| 001 - CONTROL NUMBER |
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| control field |
vtls000103180 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
KUKTEM |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20251117113349.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
180329s2018 my da f am 000 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
THE0000197(Local) |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
THE0009016(Local) |
| Qualifying information |
hardback |
| 039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE] |
|---|
| Level of rules in bibliographic description |
201905141007 |
| Level of effort used to assign nonsubject heading access points |
nazirah |
| Level of effort used to assign subject headings |
201904161247 |
| Level of effort used to assign classification |
nazri |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
UMP |
| Language of cataloging |
eng |
| Transcribing agency |
UMP |
| Description conventions |
rda |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) |
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| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) |
FIST .R64 2018 r Thesis |
| 100 0# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Nik Rohani Nik Mustapa, |
| Relator term |
author. |
| 245 10 - TITLE STATEMENT |
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| Title |
Synthesis and characterisation of metal ion-imprinted polymers for separation of rare earth elements / |
| Statement of responsibility, etc. |
Nik Rohani Nik Mustapa |
| 246 03 - VARYING FORM OF TITLE |
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| Title proper/short title |
Synthesis and characterisation of metal ion-imprinted polymers for separation of selective rare earth elements |
| 264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
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| Place of production, publication, distribution, manufacture |
Kuantan, Pahang : |
| Name of producer, publisher, distributor, manufacturer |
UMP, |
| Date of production, publication, distribution, manufacture, or copyright notice |
2018 |
| 264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
|---|
| Date of production, publication, distribution, manufacture, or copyright notice |
© 2018 |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
xvii, 85 pages : |
| Other physical details |
illustrations (some color), chart ; |
| Dimensions |
30 cm. + |
| Accompanying material |
1 CD-ROM |
| 336 ## - CONTENT TYPE |
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| Content type term |
text |
| Source |
rdacontent |
| 336 ## - CONTENT TYPE |
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| Content type term |
text |
| Source |
rdacontent |
| 337 ## - MEDIA TYPE |
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| Media type term |
unmediated |
| Source |
rdamedia |
| 337 ## - MEDIA TYPE |
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| Media type term |
computer |
| Source |
rdamedia |
| 338 ## - CARRIER TYPE |
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| Carrier type term |
volume |
| Source |
rdacarrier |
| 338 ## - CARRIER TYPE |
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| Carrier type term |
computer disc |
| Source |
rdacarrier |
| 347 ## - DIGITAL FILE CHARACTERISTICS |
|---|
| File type |
text file |
| Encoding format |
PDF |
| Source |
rda |
| 500 ## - GENERAL NOTE |
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| General note |
Faculty of Industrial Sciences and Technology |
| 502 ## - DISSERTATION NOTE |
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| Dissertation note |
Thesis (Master of Science) -- Universiti Malaysia Pahang – 2018 |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc. note |
Includes bibliographical references |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc. |
Ion imprinted polymers (IIPs) have received much attention in diverse fields owing to their high selectivity for targeted metal ions. In the present study, lanthanide-ion imprinted polymers (L-IIPs) were synthesised by dissolving stoichiometric amounts of lanthanum ion and selected complexing agents either Schiff bases, azobenzene base ligands and also indole compounds with solvent in the presence of cross-linking agent (ethylene glycol dimethacrylate (EGDMA)), functional monomer (4-vinylpyridine), and initiator (2,2-azobisisobutyronitrile (AIBN)). The cavities in the polymer materials corresponding to the specific lanthanide ions were created by leaching the polymer using aqueous HCl solution after polymerization. The complete removal of the lanthanide ions from the L-IIPs were confirmed by ICP-MS, FESEM and solid state analysis by UV-vis NIR spectroscopy. FTIR study confirmed the complexation between the L-IIPs and lanthanide ions through the nitrogen, hydroxyl oxygen and sulphur of Schiff base, azobenzene base ligands and indole compounds. At optimum (pH 6), the maximum sorption capacity achieved by the L-IIPs are estimated to be La-IIP-Schiff (25.0 mg g-1), La-IIP-Azo (24.3 mg g-1), Ce-IIP-Schiff (24.5 mg g-1), Ce-IIP-Azo (24.7 mg g-1), Pr-IIP-Schiff (125.3 mg g-1), Nd-IIP-Schiff (126.5 mg g-1), Sm-IIP-Schiff (127.6 mg g-1), Eu-IIP-Schiff (128.2 mg g-1) and Gd-IIP-Schiff (129.1 mg g-1). In the selectivity study, the L-IIPs were found to show good selectivity to the praseodymium, gadolinium, europium, samarium, cerium, neodymium and lanthanum ion in the presence of coexisting cation, promethium. It was found that imprinting results increased the affinity of the material toward several lanthanide ions over other competitor metal ions with the same charge and similar ionic radii. The synthesized L-IIPs were repeatedly used and regenerated for 8 times without a significant decrease in polymer binding affinity. |
| 610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME |
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| Corporate name or jurisdiction name as entry element |
Faculty of Industrial Sciences and Technology |
| General subdivision |
Dissertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
Universities and colleges |
| General subdivision |
Disertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name entry element |
Theses |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
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| Source of classification or shelving scheme |
Library of Congress Classification |
| Koha item type |
Thesis |