MARC details
| 000 -LEADER |
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| fixed length control field |
03067ntm a2200277 a 4500 |
| 001 - CONTROL NUMBER |
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| control field |
vtls000101428 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
KUKTEM |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20251117113357.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
171002s2017 my da f am 000 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
THE0001054(Local) |
| 039 #9 - LEVEL OF BIBLIOGRAPHIC CONTROL AND CODING DETAIL [OBSOLETE] |
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| Level of rules in bibliographic description |
201905171312 |
| Level of effort used to assign nonsubject heading access points |
nazirah |
| -- |
201710021144 |
| -- |
saini |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
UMP |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) |
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| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) |
FKKSA .Z84 2017 r Thesis |
| 100 0# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Mohammad Zuhaili Yahya |
| 245 10 - TITLE STATEMENT |
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| Title |
Synthesis and optimization of poly (HEMA-co-EGDMA-co-VBC) for preparation of hypercrosslinked aminated polymer using DoE method / |
| Statement of responsibility, etc. |
Mohammad Zuhaili Yahya |
| 260 ## - PUBLICATION, DISTRIBUTION, ETC. |
|---|
| Place of publication, distribution, etc. |
Kuantan, Pahang : |
| Name of publisher, distributor, etc. |
UMP, |
| Date of publication, distribution, etc. |
2017 |
| 300 ## - PHYSICAL DESCRIPTION |
|---|
| Extent |
xvi, 132 p. : |
| Other physical details |
ill. (some col.) ; |
| Dimensions |
30 cm. + |
| Accompanying material |
1 CD-ROM |
| 500 ## - GENERAL NOTE |
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| General note |
Faculty of Chemical & Natural Resources Engineering |
| 502 ## - DISSERTATION NOTE |
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| Dissertation note |
Thesis (Master of Science in Chemical Engineering) -- Universiti Malaysia Pahang – 2017 |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc. note |
Bibliography : p. 116-128 |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc. |
Hydrophilic quarternary ammonium resin (HQAR) was successfully derived from hypercrosslinked Poly(HEMA-co-EGDMA-co-VBC) polymer. The objective of this project is to develop HQAR via three stages, precursor synthesis (suspension polymerization), hypercrosslinking reaction, and functionalization reaction (amination). For first stage which suspension polymerization, several parameters were varied which were solvent mixture, solvent/porogen ratio, stirrer rotation, amount of initiator, amount of stabilizer, amount of crosslinker, amount of co-monomer and monomer concentration. To obtain highest quality particles, amount of crosslinker should being used at highest amount. Effect of crosslinker, co-monomer amount and monomer concentration were chosen for screening part using Design of Experiment (DoE) to study the interaction between these three factors. DoE analysis showed that the most significant factor was amount of crosslinker. Meanwhile, effects of crosslinker and co-monomer amount were chosen for DoE optimization part to optimize the particles for hypercrosslinking reaction. In second stage that involved hypercrosslinking reaction, the effect of crosslinker, co-monomer amount and catalyst ratio on particles specific surface area (SSA) were studied. Co-monomer and crosslinker amount to be significant parameters in order to obtain high SSA particles. Optimized precursors were chosen for optimization of hypercrosslinked polymer. In the last stage of this study, the optimized hypercrosslinked polymer was functionalized with Dimethylbutylamine (DMBA) to produce HQAR with positively charge group successfully attached to the backbone. The characterization involved in all stages were Scanning Electron Microscope (SEM), Fourier Transform Infrared Spectrospcopy (FTIR), X-ray Flourescence (XRF), CHNS analysis, Brunauer-Emmet-Teller (BET) and Thermal Gravimetric Analysis (TGA) |
| 610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME |
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| Corporate name or jurisdiction name as entry element |
Faculty of Chemical & Natural Resources Engineering |
| General subdivision |
Dissertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
Universities and Colleges |
| General subdivision |
Dissertations |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
|---|
| Topical term or geographic name entry element |
Theses |