Microwave assisted extraction (MAE) of beta-sitosterol from plant legumes pod / (Record no. 91104)

MARC details
000 -LEADER
fixed length control field 03463ntm a2200373 i 4500
003 - CONTROL NUMBER IDENTIFIER
control field MY-KuUP
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251125105422.0
006 - FIXED-LENGTH DATA ELEMENTS--ADDITIONAL MATERIAL CHARACTERISTICS
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007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION
fixed length control field ta
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 191108t20192019my a|||fram|| 000 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0008409(Local)
Qualifying information hardback
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
Language of cataloging eng
Transcribing agency UMP
Description conventions rda
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) FKKSA .N675 2019 r Thesis
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Norlaili Hashim,
Relator term author.
245 10 - TITLE STATEMENT
Title Microwave assisted extraction (MAE) of beta-sitosterol from plant legumes pod /
Statement of responsibility, etc. Norlaili Hashim
264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Kuantan, Pahang :
Name of producer, publisher, distributor, manufacturer UMP,
Date of production, publication, distribution, manufacture, or copyright notice 2019
264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Date of production, publication, distribution, manufacture, or copyright notice © 2019
300 ## - PHYSICAL DESCRIPTION
Extent xii, 114 pages :
Other physical details illustrations (some color) ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
337 ## - MEDIA TYPE
Media type term unmediated
Source rdamedia
337 ## - MEDIA TYPE
Media type term computer
Source rdamedia
338 ## - CARRIER TYPE
Carrier type term volume
Source rdacarrier
338 ## - CARRIER TYPE
Carrier type term computer disc
Source rdacarrier
347 ## - DIGITAL FILE CHARACTERISTICS
File type text file
Encoding format PDF
Source rda
500 ## - GENERAL NOTE
General note Faculty of Chemical and Natural Resources Engineering
502 ## - DISSERTATION NOTE
Dissertation note Thesis (Master of Science) -- Universiti Malaysia Pahang – 2019
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references
520 3# - SUMMARY, ETC.
Summary, etc. Archidendron pauciflorum or Jering, Petai or Parkia speciosa, and Leucaena leucocephala or Petai Belalang are all known as a local delicacy to many countries in Asia and yet also have the beneficial aspect in health such as an antimicrobial, antioxidant, hypoglycaemic, antiulcer and anti-hypertension. Present studies only shows on the present of phytosteroid in the plant but not its concentration. The extraction process of beta-sitosterol performed by using Microwave-Assisted Extraction process. After the extraction process, the characterization process was done by using ultraviolet-visible spectroscopy (UV-VIS), Fourier transform infrared (FTIR), high-performance liquid chromatographic analysis (HPLC) and scanning electron microscope (SEM). UV-Vis analysis analyse concentration of beta-sitosterol content in the legume pod while the FTIR will give the functional group of the legume pod. SEM shows the condition of plant surface before and after the extraction process and to ensure the extraction process at desired parameter condition. In order to optimize the maximum yield extraction of beta-sitosterol, the extraction parameter was optimize by using response surface method (RSM) by using Design Expert 7.0. The optimization process was done by using one factor at a time (OFAT) for the screening process where the research will be continued with legume pod that content with the highest yield of beta-sitosterol, fractional factorial design (FFD) for screening extraction process parameter and central composite design (CCD) for the optimization of the extraction process will be required in order to plan and investigate the most required processes. OFAT process was done by using four parameters, which are extraction duration, irradiation power, solvent concentration and extraction temperature with all three types of plant. From OFAT study result, FFD was continued with time and solvent concentration with only L. leucocephala legume. CCD result was optimized with 62.5% ethanol solvent, 7.45 min of extraction duration, 600W irradiation power and 75ºC irradiation temperature to give the highest yield of beta-sitosterol which is 0.31 mg/mL.
610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Faculty of Chemical and Natural Resources Engineering
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Universities and colleges
General subdivision Disertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Theses
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme Library of Congress Classification
Koha item type Thesis
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Collection Home library Current library Shelving location Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost Library of Congress Classification     Reference UMPLIB GAMBANG UMPLIB GAMBANG Reference 08/11/2019   FKKSA .N675 2019 r Thesis 0000127337 08/11/2019 1 08/11/2019 Thesis
  Not lost Library of Congress Classification     Reference UMPLIB GAMBANG UMPLIB GAMBANG   08/11/2019   CD12147 0000127338 26/10/2020 1 08/11/2019 Thesis

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