Study on the extraction of high methoxyl pectin from dragon fruit (hylocereus polyrhizus) peels and its adsorption performance againts cholesterol / (Record no. 94294)

MARC details
000 -LEADER
fixed length control field 04187ntm a2200373 i 4500
003 - CONTROL NUMBER IDENTIFIER
control field MY-KuUP
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251125105732.0
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007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION
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fixed length control field 201014t2 2 m a|||fram|| 000 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0008906(Local)
Qualifying information hardback
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
Language of cataloging eng
Transcribing agency UMP
Description conventions rda
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) FTKA .R83 2019 r Thesis
100 0# - MAIN ENTRY--PERSONAL NAME
Personal name Rubaiyi Mat Zaid,
Relator term author.
245 10 - TITLE STATEMENT
Title Study on the extraction of high methoxyl pectin from dragon fruit (hylocereus polyrhizus) peels and its adsorption performance againts cholesterol /
Statement of responsibility, etc. Rubaiyi Mat Zaid
264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Kuantan, Pahang :
Name of producer, publisher, distributor, manufacturer UMP,
Date of production, publication, distribution, manufacture, or copyright notice 2019
264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Date of production, publication, distribution, manufacture, or copyright notice © 2019
300 ## - PHYSICAL DESCRIPTION
Extent xvii, 173 pages :
Other physical details illustrations (some color) ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
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Content type term text
Source rdacontent
337 ## - MEDIA TYPE
Media type term unmediated
Source rdamedia
337 ## - MEDIA TYPE
Media type term computer
Source rdamedia
338 ## - CARRIER TYPE
Carrier type term volume
Source rdacarrier
338 ## - CARRIER TYPE
Carrier type term computer disc
Source rdacarrier
347 ## - DIGITAL FILE CHARACTERISTICS
File type text file
Encoding format PDF
Source rda
500 ## - GENERAL NOTE
General note Faculty of Civil Engineering Technology
502 ## - DISSERTATION NOTE
Dissertation note Thesis (Doctor of Philosophy in Civil Engineering Technology) -- Universiti Malaysia Pahang – 2019
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references
520 3# - SUMMARY, ETC.
Summary, etc. Pectin is a high value soluble dietary fiber which is beneficial to health. Requirement to manufacture the high yield of pectin with certain characteristic is a major challenge. Pectin characteristic is the keywords to its application. The purpose of this study is to investigate the extraction of hydrophobic polysaccharide which is known as high methoxyl pectin extracted from Hylocereus polyrhizus peels as potential hypolipidemic agents by in vitro sorption experiments on model molecules (cholesterol). In this study, combination of physical and chemical treatment has been applied in the extraction process. Mild ultrasonic by sonicator bath and agitation by propeller with citric acid as an extraction solvent was employed in the extraction process to achieve the high yield of high methoxyl pectin. A study on the extraction parameters (agitation rate, temperature, time, pH and liquid-solid ratio (LSR)) was performed by one-factor-at-a-time (OFAT) to facilitate the appropriate range for further optimization process. The extraction process kinetics has been done after OFAT study which would give the idea for process forecasting and optimization of the pectin yield. The kinetic analysis by Panchev’s model shows that the extraction rate was found highest at LSR 10 v/w with ymax 30.85 %. The calculated activation energy for pectin dissolution and degradation was found to be 4.532 kJ/mol and 28.054 kJ/mol, respectively. The initial screening using 25 full factorial design indicated that temperature, time, pH and LSR were significant factors in the extraction of high yield of high methoxyl pectin. All the significant factors were then optimized using response surface methodology (RSM) to achieve the high yield of high methoxyl pectin. The value of pectin yield and degree of esterification (DE) after optimization were 30.11 % and 55.00 %, respectively as compared to the initial pectin yield and DE of 21.52 % and 56.1 %, respectively. High methoxyl pectin extracted from Hylocereus polyrhizus peels (HMPHPP) were tested as potential cholesterol-lowering agent and compared with the commercial high methoxyl citrus pectin (HMPCP). The cholesterol sorption was measured quantitatively by high performance liquid chromatography (HPLC). It was found that high methoxyl pectin from Hylocereus polyrhizus peels has the affinity towards cholesterol which followed the Freundlich isotherm and pseudo-first order model. Hydrophobicity and surface structure of the HPP was characterized by contact angle analysis and field emission scanning electron microscopy (FESEM) in order understand HMPHPP surface that help the adsorption process. This study proves that high methoxyl pectin extracted from Hylocereus polyrhizus peels has affinity towards cholesterol which help the adsorption of cholesterol.
610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Faculty of Civil Engineering Technology
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Universities and colleges
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Theses
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme Library of Congress Classification
Koha item type Thesis
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Collection Home library Current library Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost Library of Congress Classification   Not for loan Reference UMPLIB GAMBANG UMPLIB GAMBANG 14/10/2020   FTKA .R83 2019 r Thesis T000000892 15/03/2021 1 14/10/2020 Thesis
  Not lost Library of Congress Classification     Reference UMPLIB GAMBANG UMPLIB GAMBANG 14/10/2020   CD12673 T000000893 06/12/2021 1 14/10/2020 Thesis

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