Synthesis of modified rice husk activated carbon and study on their carbon dioxide (co2) adsorption capacity / (Record no. 96580)

MARC details
000 -LEADER
fixed length control field 03887ntm a2200361 i 4500
003 - CONTROL NUMBER IDENTIFIER
control field MY-KuUP
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20251125110003.0
006 - FIXED-LENGTH DATA ELEMENTS--ADDITIONAL MATERIAL CHARACTERISTICS
fixed length control field t||||fr|||| 000 0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 220328s2021 my a|||frm||| 00| 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number THE0009187(Local)
Qualifying information hardback
040 ## - CATALOGING SOURCE
Original cataloging agency UMP
Language of cataloging eng
Transcribing agency UMP
Description conventions rda
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) FTKKP .A37 2021 r Thesis
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Siti Noraishah Masoum Raman,
Relator term author.
245 10 - TITLE STATEMENT
Title Synthesis of modified rice husk activated carbon and study on their carbon dioxide (co2) adsorption capacity /
Statement of responsibility, etc. Siti Noraishah Masoum Raman
264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Kuantan, Pahang :
Name of producer, publisher, distributor, manufacturer UMP,
Date of production, publication, distribution, manufacture, or copyright notice 2021
264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Date of production, publication, distribution, manufacture, or copyright notice © 2021
300 ## - PHYSICAL DESCRIPTION
Extent vii, 94 pages :
Other physical details illustrations (some color) ;
Dimensions 30 cm. +
Accompanying material 1 CD-ROM
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
336 ## - CONTENT TYPE
Content type term text
Source rdacontent
337 ## - MEDIA TYPE
Media type term unmediated
Source rdamedia
337 ## - MEDIA TYPE
Media type term computer
Source rdamedia
338 ## - CARRIER TYPE
Carrier type term volume
Source rdacarrier
338 ## - CARRIER TYPE
Carrier type term computer disc
Source rdacarrier
347 ## - DIGITAL FILE CHARACTERISTICS
File type text file
Encoding format PDF
Source rda
500 ## - GENERAL NOTE
General note Faculty of Chemical and Process Engineering Technology
502 ## - DISSERTATION NOTE
Dissertation note Thesis (Master of Science) -- Universiti Malaysia Pahang – 2021
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references
520 3# - SUMMARY, ETC.
Summary, etc. Characterization studies of impregnated activated carbon with monoethanolamine (MEA), diethanolamine (DEA), and piperazine as potential carbon dioxide (CO2) adsorbent were conducted. The adsorption capacity of the activated carbon can be increased by introducing amine group on the surface of the adsorbent. MEA, DEA, and piperazine were selected as amino compounds for the binding process on activated carbon surface. The synthesis of impregnated activated carbon was prepared according to concentration and mixture ratio. The physicochemical properties of impregnated activated carbon were characterized by x-ray diffraction (XRD), Brunauer, Emmett and Teller (BET), fourier transform infrared spectroscopy (FTIR) and field emission scanning electron microscopy (FESEM). The XRD analysis was used to determine the type of compound present on the activated carbon surface. The result revealed that the diffraction angles around 21.54º to 22.18º were linked for pyrazole, ethanolamine, diethanolamine, and benzalazine which prove the presence of hydrocarbon and amine on the activated carbon surfaces. From the BET analysis, the total surface area and pore volume decreased with increase in concentration of alkanolamine. The presence of amide functional groups in FTIR analysis at 3288 cm-1and 1651 cm-1band for the impregnated activated carbon proved that a reaction occured between carboxyl groups on the activated carbon surfaces with amine bonded. As for FESEM analysis, it was shown that the morphology of the non-impregnated activated carbon contained many pores on its surface while the pores on the impregnated activated carbon with alkanolamine were filled with amines according to the selected concentration. The sample chosen for CO2 adsorption capacity study was of the highest concentration and mixture ratio of piperazine, namely 75 wt.% and 1:2 activated carbon to piperazine ratio, respectively. The CO2 adsorption capacity studies show that the best condition for adsorption process to take place was at bed temperature of 25°C and feed gas flow rate of 20 ml/min. The CO2 uptake was highest at this temperature and flow rate for piperazine impregnated activated carbon followed by the regenerated sample and non-impregnated activated carbon which were 145.42, 95.81, and 42.00 mg-CO2/g-adsorbent respectively. The regeneration recovery for the piperazine impregnated activated carbon was more than 65%.
610 20 - SUBJECT ADDED ENTRY--CORPORATE NAME
Corporate name or jurisdiction name as entry element Faculty of Chemical and Process Engineering Technology
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Universities and colleges
General subdivision Dissertations
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Theses
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme Library of Congress Classification
Koha item type Thesis
Holdings
Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Collection Home library Current library Shelving location Date acquired Total checkouts Full call number Barcode Date last seen Copy number Price effective from Koha item type
  Not lost Library of Congress Classification   Not for loan Reference UMPLIB GAMBANG UMPLIB GAMBANG Reference 25/01/2022   FTKKP .A37 2021 r Thesis T000001763 18/05/2022 1 25/01/2022 Thesis
  Not lost Library of Congress Classification   Not for loan Reference UMPLIB GAMBANG UMPLIB GAMBANG Reference 28/03/2022   CD13049 T000001764 30/01/2023 1 28/03/2022 Thesis

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