Study on the effect of clay loading under normal and auto-thermal extrusion to the morphology structure and thermal properties of nylon 6 nanocomposites / Geraldine Chan Sue Ching

By: Material type: TextTextPublication details: Kuantan, Pahang : UMP, 2013Description: xii, 81 p. : ill. ; 30 cm. + 1 CD-ROMISBN:
  • THE0002157(Local)
Subject(s): Dissertation note: Project paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang – 2013 Abstract: In this research, the influence of auto-thermal extrusion on the thermal stability and morphology of fabricated polyamide6 (PA6) nanocomposites with varying clay loading and screw speed is discussed. The effect of zero-heat transferred extrusion systems on the thermal degradation rate of organic polymer and inorganic nanoclay is the main focus of this research. A polymer nanocomposite based from polyamide 6 and Cloisite® 20A, commercialized organic modified nanoclay, was prepared by using auto-thermal and conventional melt extrusion system. The morphological characteristics were determined through the application of X-ray diffraction (XRD) and scanning electron microscope (SEM). The thermal stability of compounded PA6/C20A nanocomposite was conducted using thermogravimetric analysis (TGA). The clay content and screw speed of the extruder dictates the quality of the PA6/C20A nanocomposites as well as the auto-thermal or conventional extrusion system itself. The auto-thermal extrusion affects the thermal stability of the melt-processed polymer nanocomposites by allowing even distribution of heat energy throughout the molten compound. However, it has very little effect on the morphology structure of PA6/C20A nanocomposites. As an addition, the screw speed of the extruder also affects the onset degradation temperature of samples produced.
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Item type Current library Call number Copy number Status Date due Barcode
Final Year Report Final Year Report UMPLIB GAMBANG QD381.9.D47 C43 2013 rs Bc. (Browse shelf(Opens below)) 1 Not for loan 0000074689
Final Year Report Final Year Report UMPLIB GAMBANG CD 7044 | QD381.9.D47 C43 2013 rs Bc. (Browse shelf(Opens below)) 1 Not for loan 0000074690

Project paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang – 2013

Bibliography : p. 68-73

In this research, the influence of auto-thermal extrusion on the thermal stability and morphology of fabricated polyamide6 (PA6) nanocomposites with varying clay loading and screw speed is discussed. The effect of zero-heat transferred extrusion systems on the thermal degradation rate of organic polymer and inorganic nanoclay is the main focus of this research. A polymer nanocomposite based from polyamide 6 and Cloisite® 20A, commercialized organic modified nanoclay, was prepared by using auto-thermal and conventional melt extrusion system. The morphological characteristics were determined through the application of X-ray diffraction (XRD) and scanning electron microscope (SEM). The thermal stability of compounded PA6/C20A nanocomposite was conducted using thermogravimetric analysis (TGA). The clay content and screw speed of the extruder dictates the quality of the PA6/C20A nanocomposites as well as the auto-thermal or conventional extrusion system itself. The auto-thermal extrusion affects the thermal stability of the melt-processed polymer nanocomposites by allowing even distribution of heat energy throughout the molten compound. However, it has very little effect on the morphology structure of PA6/C20A nanocomposites. As an addition, the screw speed of the extruder also affects the onset degradation temperature of samples produced.

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