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020 _aTHE0010075 (Local)
_qHardback
040 _aUMPSA
_beng
_cUMPSA
_erda
090 _aFTKPM .Z38 2025 r Thesis
100 0 _aWan Zateel Aqmaer Wan Ab Halim,
_eauthor.
245 1 0 _aFlexural properties of epoxy/graphene nanoplatelets nanocomposites /
_cWan Zateel Aqmaer Bt Wan Ab Halim
264 1 _aKuantan, Pahang :
_bUMPSA,
_c2025
264 4 _c© 2025
300 _axi, 52 pages :
_billustrations (some color) ;
_c30 cm. +
_e1 CD-COM
336 _2rdacontent
_atext
337 _2rdamedia
_aunmediated
338 _2rdacarrier
_avolume
347 _2rda
_atext file
_bPDF
500 _aFaculty of Manufacturing and Mechatronic Engineering Technology
502 _aThesis (Master of Science) -- Universiti Malaysia Pahang – 2025
504 _aIncludes bibliographical references
520 3 _aThis thesis reports the processing and optimization of epoxy nanocomposites reinforced graphene nanoplatelets (GNPs) to enhance flexural properties. This work aims to optimize parameters in processing epoxy and to investigate the impact of GNP loading on the properties of the resulting composites. Firstly, the parameters used to process epoxy were studied and optimized using response surface methodology (RSM). In this phase, two parameters were considered which are the rotational mixing speed in revolution per minute (rpm) of the stirrer and the curing temperature (°C) of the oven. The response for the study was set as flexural strength (MPa). From the study, it was found that the optimum parameters can be achieved at a mixing speed of 1155 rpm and 100 °C of cure temperature. These optimum parameters predict the response to be at 16.67 MPa. A verification test was performed to validate the prediction value given by the RSM and the tested sample yielded 16.57 MPa of strength for the sample prepared using those optimum parameters. These optimum parameters were used and forwarded into the second phase of the work where nanocomposites consisting of epoxy and GNPs was developed. In this stage, loading of GNPs in weight percentage (%) was varied to observe the effects of GNPs content to the whole properties of the epoxy system. As a result, it was found that the flexural strength of epoxy/GNPs nanocomposites increased relative to neat epoxy. For example, epoxy containing 4 wt.% of GNPs increased to 17.41 MPa compared to 16.57 MPa for neat epoxy but decreased to 15.74 MPa with 6wt. % GNPs. The flexural modulus also exhibited the same trend with higher modulus was observed for epoxy/GNPs compare to the modulus of neat epoxy. For example, epoxy containing 6 wt.% of GNPs increased to 6.07 GPa compared to 5.19 GPa for neat epoxy. Morphological observation through scanning electron microscope (SEM) indicated that neat epoxy has smooth fracture surface indicating less or no obstacles from the specimen to resist the load. On the other hand, epoxy/GNP nanocomposites indicate a rougher fracture surface, suggesting that GNPs become obstacles to the load, helping to resist cracks. As a conclusion, the study reveals that inclusion of GNPs enhanced the flexural strength and modulus of epoxy, but excessive particles deteriorated the properties due to agglomeration.
610 2 0 _aFaculty of Manufacturing and Mechatronic Engineering Technology
_xDissertations
650 0 _aUniversities and colleges
_xDissertations
650 0 _aThesis
_xDissertations
942 _2lcc
_cTHESIS