000 03065ntm a2200337 i 4500
003 MY-KuUP
005 20260420185027.0
006 t||||fr|||| 000 0
007 ta
008 260420t20252025my a|||fr|||| 000 0 eng d
020 _aTHE0010483 (Local)
_qHardback
040 _aUMPSA
_beng
_cUMPSA
_erda
090 _aFIST .S95 2025 r Bc.
100 1 _aPeggy, Ngu Shi Ying,
_eauthor.
245 1 0 _aSynthesis and characteristics of biobased epoxy from vanillin /
_cPeggy Ngu Shi Ying
264 1 _aKuantan, Pahang :
_bUMPSA,
_c2025
264 4 _c© 2025
300 _axii, 52 pages :
_billustrations ;
336 _2rdacontent
_atext
337 _2rdamedia
_aunmediated
338 _2rdacarrier
_avolume
347 _2rda
_atext file
_bPDF
500 _aFaculty of Industrial Sciences and Technology
502 _aFinal Year Report (Bachelor of Applied Science of Industrial Chemistry) -- Universiti Malaysia Pahang Al-Sultan Abdullah - 2025
504 _aInclude bibliographical reference
520 3 _aIn this research, there are three objectives needed to be achieved which are investigation of percentage yield of divanillin and chemical structure of vanillin and divanillin, the synthesis process of vanillin-based epoxies by differentiate their curing time, and the study the chemical structure and solvent resistance of vanillin-based epoxies which cured for different duration. In the synthesis process, heating process, and gravity filtration is the major method to get the synthesized products which are divanillin and epoxidized divanillin. The percentage yield of divanillin is calculated by using theoretical and actual yield. Comparison between vanillin and divanillin are studied through carbon-13 Nuclear Magnetic Resonance (NMR) Spectra. The curing time of the vanillin-based epoxy resins are categorized into 1 hour and 2 hours to find out its solvent resistance to four distinct solvents. Fourier Transform Infrared Spectroscopy in Attenuated total reflectance (ATR-FTIR) is used to investigate the possible functional groups in the EDV/IPDA epoxy. In conclusion, there are similarity and difference between vanillin and divanillin due to divanillin is the synthesized product of vanillin. ATR-FTIR method in the wavenumber range of 400-4000 cm-1 can recognize the key functional groups of the epoxidized divanillin (EDV) such as epoxy groups which indicated the successfully cured process in of the EDV/IPDA epoxy. Solvent resistance of the EDV/IPDA with longer curing time is more excellent due to the crosslinking network structure is more rigid and tight than the crosslinking network structure of EDV/IPDA with 1 hour curing time. These results in these experiments provide valuable insights into the synthesis process, chemical structure, solvent resistance, and percentage yield of synthesized products.
610 2 0 _aFaculty of Industrial Sciences and Technology
_xDissertations
650 0 _aUniversities and colleges
_xDissertations
856 _uhttps://umpir.ump.edu.my/id/eprint/46119
942 _2lcc
_cPSM
999 _c104761
_d104767