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020 _aTHE0010709 (Local)
_qHardback
040 _aUMPSA
_beng
_cUMPSA
_erda
090 _aFTKKP .P48 2025 r Bc.
100 0 _aPevita Shree A/P A Segar, , ,
_eauthor.
245 1 0 _aSynthesis and characterization of large quantities of functionalized graphene from graphite using a facile bubble-exfoliation method /
_cPevita Shree A/P A Segar
264 1 _aKuantan, Pahang :
_bUMPSA,
_c2025
264 4 _c© 2025
300 _a48 pages :
_billustrations ;
336 _2rdacontent
_atext
337 _2rdamedia
_aunmediated
338 _2rdacarrier
_avolume
347 _2rda
_atext file
_bPDF
500 _aFaculty of Chemical and Process Engineering Technology
502 _aFinal Year Report (Bachelor of Chemical Engineering ) -- Universiti Malaysia Pahang Al-Sultan Abdullah - 2025
504 _aInclude bibliographical reference
520 3 _aGraphene, a two-dimensional allotrope of carbon, has garnered significant interest due to its exceptional mechanical strength, thermal and electrical conductivity, and potential applications in various industries. Despite its promising characteristics, the large-scale production of graphene remains a challenge due to limitations in current synthesis methods. This study explores the synthesis of graphene from graphite flakes using a novel bubble exfoliation technique aided by liquid-phase exfoliation in ethanol. This method leverages cavitation bubbles generated through ultrasonication to facilitate the separation of graphene layers, offering a scalable and environmentally friendly alternative to conventional methods. The research focuses on optimizing the synthesis parameters, specifically the sonication time and the solvent-to-graphite ratio, to enhance the yield and quality of the produced graphene sheets. In this work, a significant amount of graphene was synthesized in a short time with a fixed frequency and temperature of the sonication. Fourier-transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), and Ultraviolet-visible spectroscopy (UV–Vis) techniques validated the oxidation effect of the synthesis process on graphene, which is in line with the addition of functional groups to it. Besides, XRD characterizations showed that graphene mainly consists of a thin few-layer structure. Furthermore, FTIR and Uv-Vis revealed that the functional group that exists in the synthesized graphene are primarily hydroxyl groups. Thus, this research aims to contribute to the understanding and optimization of bubble exfoliation as a scalable and environmentally friendly method for graphene production. By overcoming the limitations of current exfoliation techniques, this study seeks to advance the practical applications of graphene in various industries and support its anticipated market growth.
610 2 0 _aFaculty of Chemical and Process Engineering Technology
_xDissertations
650 0 _aUniversities and colleges
_xDissertations
650 0 _aTheses
_xDissertations
856 _uhttps://umpir.ump.edu.my/id/eprint/47587
942 _2lcc
_cPSM
999 _c105178
_d105184