| 000 | 02013nam a2200253 a 4500 | ||
|---|---|---|---|
| 001 | vtls000067873 | ||
| 003 | KUKTEM | ||
| 005 | 20251114204526.0 | ||
| 008 | 121219t2012 my a f m 000 0 eng d | ||
| 020 | _aTHE0004057(Local) | ||
| 039 | 9 |
_a201905160858 _bfauzi _y201212191633 _zFida |
|
| 040 | _aUMP | ||
| 090 | _aTP156.E8 N67 2012 rs Bc. | ||
| 100 | 0 | _aNorhamizah Johari | |
| 245 | 1 | 0 |
_aBatch extraction of 1,3,7-trymethylxanthine from KKM22 cocoa seeds / _cNorhamizah Johari |
| 260 |
_aKuantan, Pahang : _bUMP, _c2012 |
||
| 300 |
_axiii, 38 p. : _bill. ; _c30 cm. + _e1 CD-ROM |
||
| 502 | _aProject paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang - 2012 | ||
| 504 | _aBibliography : p. 27-29 | ||
| 520 | 3 | _a1,3,7- trymethylxanthine (caffeine) is a naturally occurring substance found in cocoa seeds. The purpose of this research is to extract caffeine from Klon Koko Malaysia (KKM)22, to investigate the effect of particle size, solvent/feed ratio and extraction time, and also to determine the kinetic model for extraction of 1,3,7-trymethylxantine. The sample was prepared by grinding and sieving, followed by solid-liquid extraction using water by heat reflux extracting technique, liquid-liquid extraction with ethyl acetate, drying of caffeine by rotary evaporator, and finally analysis of the caffeine yield. The analysis of the caffeine yield was done using UV/Vis Spectrophotometric method. The caffeine yield was highest at sample particle size of 315 μm (0.22 % w/w caffeine or 2.1724 mg/g cocoa), solvent/feed ratio of 1:1 (0.22 % w/w caffeine or 2,2102 mg/g cocoa), and extraction time of 90 minutes (0.23 % w/w caffeine or 2.288 mg/g cocoa). The best conditions for the highest yield of caffeine from KKM22 were 315 μm of sample particle size, 1:1 of solvent/feed ratio, and 90 minutes of extraction time. | |
| 650 | 0 | _aExtraction (Chemistry) | |
| 650 | 0 | _aCaffeine | |
| 999 |
_aVIRTUA40 _c3542 _d3548 |
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| 999 | _aVTLSSORT0080*0200*0400*0900*1000*2450*2600*3000*5020*5040*5200*6500*6501*9992 | ||