000 03633ntm a2200373 i 4500
001 vtls000102846
003 KUKTEM
005 20251117113351.0
008 180124s2017 my da f a m 000 0 eng d
020 _aTHE0000832(Local)
039 9 _a201905271215
_bnazirah
_c201802081554
_dfateeha
_c201802021701
_dfateeha
_y201801241042
_zfateeha
040 _aUMP
_beng
_cUMP
_erda
090 _aFKKSA .A379 2017 r Bc.
100 0 _aSiti Aisyah Abdull Malid,
_eauthor.
245 1 0 _aSupported liquid membrane for acetic acid extraction :
_bscreening of membrane support preparation factors /
_cSiti Aisyah Abdull Malid
264 1 _aKuantan, Pahang :
_bUMP,
_c2017
264 4 _c© 2017
300 _axiv, 50 pages :
_billustrations (some color), charts ;
_c30 cm. +
_e1 CD-ROM
336 _atext
_2rdacontent
336 _atext
_2rdacontent
337 _aunmediated
_2rdamedia
337 _acomputer
_2rdamedia
338 _avolume
_2rdacarrier
338 _acomputer dics
_2rdacarrier
347 _atext file
_bPDF
_2rda
500 _aFaculty of Chemical & Natural Resources Engineering
502 _aProject Paper (Bachelor of Chemical Engineering) -- Universiti Malaysia Pahang – 2017
504 _aIncludes bibliographical references
520 3 _aLignocellulosic materials can be acid hydrolyzed into fermentable sugars for ethanol production. However, inhibitory compounds such as carboxylic acid, furans and phenolic substances are also generated during this process. It is necessary to separate these inhibitors from the sugars or to reduce their concentration prior to the fermentation process in order to maximize the ethanol yields. This work focused on the removal of the acetic acid from biomass hydrolysate using supported liquid membrane (SLM) process. The membrane support for the SLM system was fabricated from 15wt% PES, 42.5wt% DMAc, 42.5wt% PEG 200 and 0.1wt% graphene by using vapour-induced phase separation (VIPS) method. Tri-n-octylamine (TOA) and 2-ethyl hexanol were used as carrier and solvent respectively in organic liquid membrane formulation. Two level full factorial design (FFD) was employed to perform the screening of three factors during VIPS process which are temperature of water bath (A) (30-60⁰C), exposure time (B) (10-60 seconds) and air humidity (C) (70-90%). The response was evaluated based on acetic acid extraction percentage from 10 g/L aqueous acetic acid feed solution. From the screening result, all three main factors were significant to the SLM performance. Air humidity factor (C) gave the highest contribution of 28.96% among the main factors. In term of the interaction between factors, water bath temperature (A) and exposure time (B) give the most significant effect with 45.01% percentage of contribution. The second highest interaction effect with 13.20% contribution was the interaction between air exposure time (B) and air humidity (C), however the interaction graph is not intercept. Meanwhile, the interaction effect of water bath temperature (A) and air humidity (C) is insignificant as extraction of acetic acid decrease as both factors were increased. The highest extraction percentage for the acetic acid using SLM system was 75.95% which is using the membrane prepare at 30⁰C water bath temperature, 10 seconds exposure time and 70% air humidity.
610 2 0 _aFaculty of Chemical & Natural Resources Engineering
_xDissertations
650 0 _aUniversities and Colleges
_xDissertations
650 0 _aTheses
999 _aVIRTUA40
_c7444
_d7450
999 _aVTLSSORT0080*0200*0400*0900*1000*2450*2640*2641*3000*3360*3361*3370*3371*3380*3381*3470*5000*5020*5040*5200*6100*6500*6501*9992