Biodiesel production via two steps catalyzed process : the study on effect of temperature and catalyst weight percent to the biodiesel yield, FFA content and acid value / Amminatul Farhayu Abdul Talib

By: Material type: TextTextPublication details: Kuantan, Pahang : UMP, 2008Description: 60 p. : ill. ; 30 cm. + 1 computer discISBN:
  • THE0004592(Local)
Other title:
  • Biodiesel production via two steps catalyzed process : the study on effect of temperature and catalyst weight percent to the biodiesel yield, FFA content and acid value [electronic resource]
Subject(s): Dissertation note: Project paper (Bachelor of Chemical Engineering) --- Universiti Malaysia Pahang - 2008 Abstract: In this study, the effects of temperature and catalyst weight percent to the biodiesel yield, FFA content and acid value were studied. The biodiesel is produced by two-steps catalyzed process. The essential part of the process is the transesterification of waste cooking oil (WCO) with methanol in present of catalyst, to yield methyl ester as the main product and glycerin as the by-product. In the acid treatment or the acid- catalyzed esterification, the temperature is set at 95°C, acid catalyst of 2%w/wH2SO and methanol to waste cooking oil of 10:1. For the alkali-catalyzed transesterification, the range of temperature is 40°C-80°C, the alkali c atalyst weight percent is varied from 0.2 to 1.0%wNaOH/wWCO. The ultrasonic wave and ratio of methanol to waste cooking was fixed at 32MHz and 6:1 respectively. The biodiesel product is then analyzed by titration to check the FFA content and the acid value. The best temperature and alkali catalyst weight percent was found at 70° C and 1.0%wNaOH/wWCO correspondingly. The total reduction of FFA content after acid treatment was 36.92%. The two steps catalyzed process is preferable for raw material that has high content of FFA such as waste cooking oil. -Author
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Item type Current library Call number Copy number Status Date due Barcode
Final Year Report Final Year Report UMPLIB GAMBANG TP359.B46 A46 2008 rs Thesis (Browse shelf(Opens below)) 1 Not for loan 0000031367
Final Year Report Final Year Report UMPLIB GAMBANG CD 2747 | TP359.B46 A46 2008 rs Thesis (Browse shelf(Opens below)) 1 Not for loan 0000031368

Project paper (Bachelor of Chemical Engineering) --- Universiti Malaysia Pahang - 2008

In this study, the effects of temperature and catalyst weight percent to the biodiesel yield, FFA content and acid value were studied. The biodiesel is produced by two-steps catalyzed process. The essential part of the process is the transesterification of waste cooking oil (WCO) with methanol in present of catalyst, to yield methyl ester as the main product and glycerin as the by-product. In the acid treatment or the acid- catalyzed esterification, the temperature is set at 95°C, acid catalyst of 2%w/wH2SO and methanol to waste cooking oil of 10:1. For the alkali-catalyzed transesterification, the range of temperature is 40°C-80°C, the alkali c atalyst weight percent is varied from 0.2 to 1.0%wNaOH/wWCO. The ultrasonic wave and ratio of methanol to waste cooking was fixed at 32MHz and 6:1 respectively. The biodiesel product is then analyzed by titration to check the FFA content and the acid value. The best temperature and alkali catalyst weight percent was found at 70° C and 1.0%wNaOH/wWCO correspondingly. The total reduction of FFA content after acid treatment was 36.92%. The two steps catalyzed process is preferable for raw material that has high content of FFA such as waste cooking oil. -Author

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